The changes of transmission electron diffraction patterns indicate the phase change has occurred at about 220k, and its crystal parameters change obviously.
透射电子衍射花样的变化表明在220k附近发生了相变，它的晶体结构参数明显地变化。
The resultant surfaces were characterized by means of SEM, transmission electron microscopy (TEM), X-ray diffraction (XRD), and water contact Angle measurements.
用扫描电镜、透射电镜、X射线衍射、接触角测量等技术对表面进行了表征。
X-ray diffraction and transmission electron microscope experiments indicate the powder sample is amorphous and also show the average particle size and crystallization products.
射线衍射和透射电子显微镜实验不但证实它的非晶性，而且给出它的平均颗粒度大小和晶化产物。
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